C₃₂H₃₂ClFN₄O₈S

Base Information

Chemical Name:C₃₂H₃₂ClFN₄O₈S
CAS No.:1101244-15-8
Molecular Formula:C₃₂H₃₂ClFN₄O₈S
Molecular Weight:687.145
Hs Code.:

C<sub>32</sub>H<sub>32</sub>ClFN<sub>4</sub>O<sub>8</sub>S

Synonyms:C₃₂H₃₂ClFN₄O₈S

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Chemical Property of C₃₂H₃₂ClFN₄O₈S

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Technology Process of C₃₂H₃₂ClFN₄O₈S

There total 12 articles about C₃₂H₃₂ClFN₄O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1093628-41-1
5-chloro-N-({(5S)-3-[2-fluoro-4-(3-oxomorpholin-4-yl)phenyl]-2-oxo-1,3-oxazolidin-5-yl}methyl)thiophene-2-carboxamide

: 947181-30-8
benzyl (4-chloro-4-oxobutyl)methylcarbamate

: 1101244-15-8
C₃₂H₃₂ClFN₄O₈S

Guidance literature:: 5-chloro-N-({(5S)-3-[2-fluoro-4-(3-oxomorpholin-4-yl)phenyl]-2-oxo-1,3-oxazolidin-5-yl}methyl)thiophene-2-carboxamide; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

benzyl (4-chloro-4-oxobutyl)methylcarbamate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

Reference yield:

: 29632-74-4
2-fluro-4-iodoaniline

: 1101244-15-8
C₃₂H₃₂ClFN₄O₈S

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium carbonate / dichloromethane; water / 144 h / Reflux

2.1: potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 15 h / Inert atmosphere; Reflux

3.1: hydrogen / palladium 10% on activated carbon / ethanol / 1 h / 20 °C / 750.08 Torr

4.1: magnesium(II) perchlorate / acetonitrile / 15 h / 20 °C

5.1: dmap / propyl cyanide / 72 h / 70 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

6.2: 0.25 h / 20 °C

With dmap; potassium phosphate; copper(l) iodide; magnesium(II) perchlorate; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium carbonate; N,N`-dimethylethylenediamine; palladium 10% on activated carbon; In 1,4-dioxane; propyl cyanide; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1093628-67-1
N,N-Dibenzyl-2-fluoro-4-iodoaniline

: 1101244-15-8
C₃₂H₃₂ClFN₄O₈S

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium phosphate; copper(l) iodide; N,N`-dimethylethylenediamine / 1,4-dioxane / 15 h / Inert atmosphere; Reflux

2.1: hydrogen / palladium 10% on activated carbon / ethanol / 1 h / 20 °C / 750.08 Torr

3.1: magnesium(II) perchlorate / acetonitrile / 15 h / 20 °C

4.1: dmap / propyl cyanide / 72 h / 70 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C

5.2: 0.25 h / 20 °C

With dmap; potassium phosphate; copper(l) iodide; magnesium(II) perchlorate; hydrogen; sodium hydride; N,N`-dimethylethylenediamine; palladium 10% on activated carbon; In 1,4-dioxane; propyl cyanide; ethanol; N,N-dimethyl-formamide; acetonitrile;