C₄₆H₅₆N₂O₉Si₂

Base Information

Chemical Name:C₄₆H₅₆N₂O₉Si₂
CAS No.:1410805-33-2
Molecular Formula:C₄₆H₅₆N₂O₉Si₂
Molecular Weight:837.13
Hs Code.:

C<sub>46</sub>H<sub>56</sub>N<sub>2</sub>O<sub>9</sub>Si<sub>2</sub>

Synonyms:C₄₆H₅₆N₂O₉Si₂

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Chemical Property of C₄₆H₅₆N₂O₉Si₂

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Technology Process of C₄₆H₅₆N₂O₉Si₂

There total 27 articles about C₄₆H₅₆N₂O₉Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: C₄₆H₅₆N₂O₉Si₂

: 1410805-33-2
C₄₆H₅₆N₂O₉Si₂

Guidance literature:: With copper(II) acetate monohydrate; In methanol; at 20 ℃; for 22h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol302691j

Reference yield:

: 1410805-21-8
C₂₆H₄₃NO₆Si₂

: 1410805-33-2
C₄₆H₅₆N₂O₉Si₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: diisobutylaluminium hydride / hexane; toluene / 2 h / -78 °C / Inert atmosphere

2.1: sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine / dichloromethane; dimethyl sulfoxide / 1 h / 0 °C / Inert atmosphere

3.1: pentane; diethyl ether / 0.75 h / -78 - 0 °C / Inert atmosphere

4.1: pyridine hydrogenfluoride; THF-pyridine / tetrahydrofuran / 0.75 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

5.1: acetic acid / methanol / 26 h / 0 °C / Inert atmosphere

6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; aq. phosphate buffer; acetone / 2 h / 20 °C / pH 7 / Inert atmosphere

7.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.5 h / 20 °C / pH 7 / Inert atmosphere

8.1: hydroxylamine hydrochloride; pyridine / ethanol / 1 h / 0 °C / Inert atmosphere

9.1: pyridine; N-ethyl-N,N-diisopropylamine; N-chloro-succinimide / chloroform / 44.75 h / 20 - 60 °C / Inert atmosphere

10.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

11.1: samarium diiodide / tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere

12.1: Martins sulfurane / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

13.1: methanol / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

14.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

15.1: copper(II) acetate monohydrate / methanol / 22 h / 20 °C / Inert atmosphere

With pyridine; methanol; sodium periodate; N-chloro-succinimide; osmium(VIII) oxide; samarium diiodide; THF-pyridine; Martins sulfurane; hydroxylamine hydrochloride; sulfur trioxide pyridine complex; copper(II) acetate monohydrate; diisobutylaluminium hydride; Dess-Martin periodane; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; aq. phosphate buffer; diethyl ether; ethanol; hexane; dichloromethane; chloroform; dimethyl sulfoxide; acetone; toluene; pentane; 11.1: |Reformatsky Reaction;
DOI:10.1021/ol302691j

Reference yield:

: C₂₇H₄₅NO₆Si₂

: 1410805-33-2
C₄₆H₅₆N₂O₉Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: hydroxylamine hydrochloride; pyridine / ethanol / 1 h / 0 °C / Inert atmosphere

2: pyridine; N-ethyl-N,N-diisopropylamine; N-chloro-succinimide / chloroform / 44.75 h / 20 - 60 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

4: samarium diiodide / tetrahydrofuran / 0.42 h / -78 °C / Inert atmosphere

5: Martins sulfurane / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

6: methanol / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

7: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

8: copper(II) acetate monohydrate / methanol / 22 h / 20 °C / Inert atmosphere

With pyridine; methanol; N-chloro-succinimide; samarium diiodide; Martins sulfurane; hydroxylamine hydrochloride; copper(II) acetate monohydrate; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; 4: |Reformatsky Reaction;
DOI:10.1021/ol302691j