1,3,5-tris(aminomethyl)benzene trihydrochloride

Base Information

• Chemical Name: 1,3,5-tris(aminomethyl)benzene trihydrochloride
• CAS No.: 69146-57-2
• Molecular Formula: C₉H₁₅N₃*3ClH
• Molecular Weight: 274.621

Synonyms:1,3,5-tris(aminomethyl)benzene trihydrochloride

Chemical Property of 1,3,5-tris(aminomethyl)benzene trihydrochloride

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1,3,5-Tris(Aminomethyl)benzene trihydrochloride 97% ^*data from reagent suppliers

Safty Information:

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Technology Process of 1,3,5-tris(aminomethyl)benzene trihydrochloride

There total 5 articles about 1,3,5-tris(aminomethyl)benzene trihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,3,5-tris(tert-butoxycarbonylaminomethyl)benzene → 1,3,5-tris(aminomethyl)benzene trihydrochloride (69146-57-2)

Guidance literature:

1,3,5-tris(tert-butoxycarbonylaminomethyl)benzene; With trifluoroacetic acid; In dichloromethane; Cooling with ice; Inert atmosphere;

With hydrogenchloride; In methanol; water; Inert atmosphere;

DOI:10.1002/chem.202005026

Reference yield: 53.0%

1,3,5-tris(phthalimidomethyl)-benzene (106296-54-2) → 1,3,5-tris(aminomethyl)benzene trihydrochloride (69146-57-2)

Guidance literature:

With hydrogenchloride; hydrazine hydrate; In ethanol; toluene; for 72h; Heating;

DOI:10.1021/ol9910924

Reference yield:

1,3,5-Tris(bromomethyl)benzene (18226-42-1) → 1,3,5-tris(aminomethyl)benzene trihydrochloride (69146-57-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 71 percent / 18-crown-6 / toluene / 24 h / 100 °C

2: 53 percent / hydrazyne hydrate; HCl / ethanol; toluene / 72 h / Heating

With hydrogenchloride; 18-crown-6 ether; hydrazine hydrate; In ethanol; toluene; 1: Condensation / 2: Disproportionation;

DOI:10.1021/ol9910924

upstream raw materials:

tetrabutyl-ammonium chloride

1,3,5-tris(phthalimidomethyl)-benzene

1,3,5-Tris(bromomethyl)benzene

1,3,5-tricyanobenzene

Downstream raw materials:

1,3,5-tris<<(2,3-dimethoxy-4-methylbenzoyl)amino>methyl>benzene

N,N',N''-tris(2-methoxybenzoyl)-1,3,5-tris(aminomethyl)benzene

N,N',N''-tris(2-hydroxybenzoyl)-1,3,5-tris(aminomethyl)benzene

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