β-apo-8'-carotenal

Base Information

Chemical Name:β-apo-8'-carotenal
CAS No.:5056-12-2
Molecular Formula:C₃₅H₄₆O
Molecular Weight:482.75
Hs Code.:

Synonyms:β-apo-8'-carotenal

Suppliers and Price of β-apo-8'-carotenal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-apo-8'-carotenal

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of β-apo-8'-carotenal

There total 8 articles about β-apo-8'-carotenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₂₈H₃₂BrO₂P

: 59598-23-1,367493-63-8,367493-64-9,367493-65-0,4172-46-7
8'-apo-β-carotenal

: 5056-12-2
(2E,4E,6E,8E,10E,12Z,14E,16E,18E,20E)-2,6,10,15,19-Pentamethyl-21-(2,6,6-trimethyl-cyclohex-1-enyl)-henicosa-2,4,6,8,10,12,14,16,18,20-decaenal

Guidance literature:: C₂₈H₃₂BrO₂P; 8'-apo-β-carotenal; With sodium methylate; In methanol; for 24h; Reflux;

With toluene-4-sulfonic acid; In acetone; for 2h;
DOI:10.1016/j.tet.2012.10.041

Reference yield:

: 62073-42-1
(2E,4E,6E)-8-hydroxy-2,6-dimethyl-octa-2,4,6-trienal

: 5056-12-2
β-apo-8'-carotenal

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃ / dimethylformamide; CH₂Cl₂

2: CH₂Cl₂

3: (i) HC(OMe)3, TsOH, H₃PO₄, (ii) /BRN= 1889023/, NaOMe

With phosphorus tribromide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 3950-23-0
8-acetoxy-2,6-dimethyl-octa-2,4,6-trien-1-al

: 5056-12-2
β-apo-8'-carotenal

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH / methanol

2: PBr₃ / dimethylformamide; CH₂Cl₂

3: CH₂Cl₂

4: (i) HC(OMe)3, TsOH, H₃PO₄, (ii) /BRN= 1889023/, NaOMe

With sodium hydroxide; phosphorus tribromide; In methanol; dichloromethane; N,N-dimethyl-formamide;