[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃

Base Information

• Chemical Name: [Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃
• CAS No.: 87183-73-1
• Molecular Formula: C₇H₇O₃S*C₁₀H₂₂CoN₅O₇P
• Molecular Weight: 587.478

Synonyms:[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃

Chemical Property of [Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃

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Technology Process of [Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃

There total 1 articles about [Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*C₇H₇SO₃^(1-)=[Co(NH₂CH₂CH₂NH₂)2((⁽¹⁸⁾O)H₂)(O₃POC₆H₄NO₂)]SO₃C₆H₄CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ammonium p-toluenesulfonate (4124-42-9) + [Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)](1+)*ClO4(1-)*H2O=[Co(NH2CH2CH2NH2)2(OH2)(O3POC6H4NO2)]ClO4*H2O (87183-71-9) + 18O-labeled water (14797-71-8) → [Co(NH2CH2CH2NH2)2(((18)O)H2)(O3POC6H4NO2)](1+)*C7H7SO3(1-)=[Co(NH2CH2CH2NH2)2(((18)O)H2)(O3POC6H4NO2)]SO3C6H4CH3 (87183-73-1)

Guidance literature:

With trifluorormethanesulfonic acid; ammonia; In further solvent(s); to suspn. of Co complex in (((18)O)H2) added CF3SO3H (pH 1.5), warmed to 50 .deghree.C, stirred until all of solid dissolved, allowed to stand at room temp. for 4 d, filtered, pH filtrate adjusted to 4-5 (concd. aq.NH3), added NH4SO3C6H4CH3; pptd. by cooling at 0 ° C for 2 h, ppt. washed ice-cold H2O, allowed to dry in air for 20 min, anhyd. product obtained by desication in vac. over P2O5 over 18 h; elem. anal.;

DOI:10.1021/ja00363a021

upstream raw materials:

ammonium p-toluenesulfonate

[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]⁽¹⁺⁾*ClO₄^(1-)*H₂O=[Co(NH₂CH₂CH₂NH₂)2(OH₂)(O₃POC₆H₄NO₂)]ClO₄*H₂O

¹⁸O-labeled water

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