(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Base Information

Chemical Name:(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester
CAS No.:204061-14-3
Molecular Formula:C₃₈H₄₆N₂O₅Si
Molecular Weight:638.879
Hs Code.:

Synonyms:(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

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Chemical Property of (3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

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Technology Process of (3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

There total 4 articles about (3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 204061-10-9
{3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester

: 204061-14-3
(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

: 174626-34-7
N-(benzyloxycarbonyl)-3-amino-1-propyl methanesulfonate

: 204061-14-3
(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaBr / dimethylformamide

2: 81 percent / NaI, K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

3: 93 percent / Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

4: 88 percent / Et₃N / CH₂Cl₂ / 4 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; sodium iodide; sodium bromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

: 39945-54-5
benzyl N-(3-bromopropyl)carbamate

: 204061-14-3
(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / NaI, K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: 93 percent / Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

3: 88 percent / Et₃N / CH₂Cl₂ / 4 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2