{3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester

Base Information

• Chemical Name: {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester
• CAS No.: 204061-10-9
• Molecular Formula: C₃₀H₄₀N₂O₃Si
• Molecular Weight: 504.745

Synonyms:{3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester

Chemical Property of {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester

Chemical Property:

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Technology Process of {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester

There total 3 articles about {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

tert-butylchlorodiphenylsilane (58479-61-1) + 7-(N-phenylmethoxycarbonyl)amino-4-azaheptanol (204061-09-6) → {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester (204061-10-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; for 5h; Ambient temperature;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

N-(benzyloxycarbonyl)-3-amino-1-propyl methanesulfonate (174626-34-7) → {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester (204061-10-9)

Guidance literature:

Multi-step reaction with 3 steps

1: NaBr / dimethylformamide

2: 81 percent / NaI, K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

3: 93 percent / Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; sodium iodide; sodium bromide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

Reference yield:

benzyl N-(3-bromopropyl)carbamate (39945-54-5) → {3-[3-(tert-Butyl-diphenyl-silanyloxy)-propylamino]-propyl}-carbamic acid benzyl ester (204061-10-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 81 percent / NaI, K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: 93 percent / Et₃N, DMAP / CH₂Cl₂ / 5 h / Ambient temperature

With dmap; potassium carbonate; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/(SICI)1521-3765(199801)4:1<137::AID-CHEM137>3.0.CO;2-2

upstream raw materials:

tert-butylchlorodiphenylsilane

7-(N-phenylmethoxycarbonyl)amino-4-azaheptanol

benzyl N-(3-bromopropyl)carbamate

N-(benzyloxycarbonyl)-3-amino-1-propyl methanesulfonate

Downstream raw materials:

(3-Benzyloxycarbonylamino-propyl)-[3-(tert-butyl-diphenyl-silanyloxy)-propyl]-carbamic acid benzyl ester

N¹⁶-cholesteryloxycarbonyl-4,8,13-triaza-N^1,4,13-tri(phenylmethoxycarbonyl)hexadecane-1,16-diamine

C₅₃H₈₀N₄O₆

{3-[(3-Azido-propyl)-benzyloxycarbonyl-amino]-propyl}-carbamic acid benzyl ester

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