1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone

Base Information

• Chemical Name: 1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone
• CAS No.: 1001413-15-5
• Molecular Formula: C₂₁H₂₂N₄O₄S
• Molecular Weight: 426.496

Synonyms:1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone

Chemical Property of 1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone

Chemical Property:

Purity/Quality:

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Technology Process of 1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone

There total 1 articles about 1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridine-7-carbonitrile (1001412-95-8) + methylmagnesium bromide (75-16-1) → 1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone (1001413-15-5)

Guidance literature:

3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridine-7-carbonitrile; methylmagnesium bromide; In tetrahydrofuran; at -20 ℃; for 0.666667h;

With sulfuric acid; at -20 - 20 ℃; Further stages.;

DOI:10.1021/jm070650e

Reference yield:

1-[3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]ethanone (1001413-15-5) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → 1-[3-(4-benzoyl-2-methylpiperazine-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridin-7-yl]-3-dimethylaminopropene

Guidance literature:

In N,N-dimethyl-formamide; at 55 - 60 ℃; for 6h;

DOI:10.1021/jm070650e

upstream raw materials:

3-(4-benzoyl-2-methylpiperazin-1-sulfonyl)-1H-pyrrolo[2,3-c]pyridine-7-carbonitrile

methylmagnesium bromide

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