Cyclohexane-1,2-diyldimethanediyl dimethanesulfonate

Base Information

Chemical Name:Cyclohexane-1,2-diyldimethanediyl dimethanesulfonate
CAS No.:66347-68-0
Molecular Formula:C10H20O6S2
Molecular Weight:300.397
Hs Code.:
NSC Number:170782,120389
DSSTox Substance ID:DTXSID20298043

Synonyms:cyclohexane-1,2-diyldimethanediyl dimethanesulfonate;66347-68-0;[2-(methylsulfonyloxymethyl)cyclohexyl]methyl methanesulfonate;(1S,2S)-Cyclohexane-1,2-diylbis(methylene) dimethanesulfonate;MFCD12923309;(1R,2R)-1,2-Bis[[(methylsulfonyl)oxy]methyl]cyclohexane;SCHEMBL2548198;DTXSID20298043;NSC120389;NSC170782;AKOS030613698;NSC-120389;NSC-170782;SB44578;SB49713;SY033152;FT-0665348

Suppliers and Price of Cyclohexane-1,2-diyldimethanediyl dimethanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of Cyclohexane-1,2-diyldimethanediyl dimethanesulfonate

Chemical Property:

Vapor Pressure:1.83E-09mmHg at 25°C
Boiling Point:495.3ºC at 760 mmHg
Flash Point:253.3ºC
Density:1.27g/cm3
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:300.07013070
Heavy Atom Count:18
Complexity:398

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CS(=O)(=O)OCC1CCCCC1COS(=O)(=O)C

Technology Process of Cyclohexane-1,2-diyldimethanediyl dimethanesulfonate

There total 5 articles about Cyclohexane-1,2-diyldimethanediyl dimethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 76155-27-6,25712-33-8
(+/-)-trans-2-(hydroxymethyl)cyclohexylmethanol

: 124-63-0
methanesulfonyl chloride

: 66347-68-0,139506-07-3
(±)-(1S, 2S)-cyclohexane-1,2-dimethanol bis(methanesulfonate)

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/ml400235c

Reference yield:

: 13149-00-3
1,2-cis-cyclohexanedicarboxylic anhydride

: 66347-68-0
(±)-(1S, 2R)-cyclohexane-1,2-dimethanol bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 2 h / 0 - 20 °C

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 17351-07-4,17351-22-3
diethyl cyclohexane-cis-1,2-dicarboxylate

: 66347-68-0
(±)-(1S, 2R)-cyclohexane-1,2-dimethanol bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄; diethyl ether

2: pyridine

With pyridine; lithium aluminium tetrahydride; diethyl ether;
DOI:10.1039/jr9530000399