2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

Base Information

Chemical Name:2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester
CAS No.:1182349-15-0
Molecular Formula:C₂₁H₂₀BrN₃O₅
Molecular Weight:474.311
Hs Code.:

Synonyms:2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

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Chemical Property of 2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

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Technology Process of 2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

There total 1 articles about 2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 96192-93-7
methyl 2-(S)-benzyloxycarbonylamino-3-aminopropionate hydrochloride

: 16732-64-2
4-bromo-1H-indole-2-carboxylic acid

: 1182349-15-0
2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

Guidance literature:: 4-bromo-1H-indole-2-carboxylic acid; With pyridine; 1,1'-carbonyldiimidazole; at 20 ℃;

methyl 2-(S)-benzyloxycarbonylamino-3-aminopropionate hydrochloride; With pyridine; at 20 ℃; for 48h;
DOI:10.1021/jm900363q

Reference yield: 97.0%

: 1182349-15-0
2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

: 1210043-01-8
C₂₀H₁₈BrN₃O₅

Guidance literature:: 2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester; With water; sodium hydroxide; In tetrahydrofuran; at 20 ℃;

With hydrogenchloride; water;
DOI:10.1021/jm900363q

Reference yield: 68.6%

: 1182349-15-0
2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester

: 98-80-6
phenylboronic acid

: 1182349-07-0
2-benzyloxycarbonylamino-3-[(4-phenyl-1H-indole-2-carbonyl)amino]propionic acid

Guidance literature:: 2-benzyloxycarbonylamino-3-[(4-bromo-1H-indole-2-carbonyl)amino]propionic acid methyl ester; phenylboronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; Reflux;

With hydrogenchloride; water;
DOI:10.1021/jm900363q