1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate

Base Information

• Chemical Name: 1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate
• CAS No.: 1218936-83-4
• Molecular Formula: C₁₇H₁₉O₆P
• Molecular Weight: 350.308
• Mol file: 1218936-83-4.mol

Synonyms:1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate

Chemical Property of 1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate

There total 1 articles about 1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl benzoylphosphonate (18106-71-3) + ortho-anisaldehyde (135-02-4) → 1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate (1218936-83-4)

Guidance literature:

With {K(18-crown-6)}CN; In diethyl ether;

DOI:10.1021/ol100410k

Reference yield: 99.0%

1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate (1218936-83-4) + methoxybenzene (100-66-3) → 2-(2-methoxyphenyl)-2-(4-methoxyphenyl)-1-phenylethanone (1218936-84-5)

Guidance literature:

1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate; methoxybenzene; In 1,2-dichloro-ethane; at 23 ℃; Inert atmosphere;

With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 23 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ol100410k

Reference yield: 84.0%

1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate (1218936-83-4) + thiophenol (108-98-5) → 2-(2-methoxyphenyl)-1-phenyl-2-(phenylthio)ethanone (1218936-86-7)

Guidance literature:

1-(2-methoxyphenyl)-2-oxo-2-phenylethyl dimethyl phosphate; thiophenol; In 1,2-dichloro-ethane; at 23 ℃; Inert atmosphere;

With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 23 ℃; for 5.5h; Inert atmosphere;

DOI:10.1021/ol100410k

upstream raw materials:

dimethyl benzoylphosphonate

ortho-anisaldehyde

Downstream raw materials:

2-(furan-2-yl)-2-(2-methoxyphenyl)-1-phenylethanone

2-(o-methoxyphenyl)-1,4-diphenyl-1,4-butanedione

2-(2,5-dimethylphenyl)-2-(2-methoxyphenyl)-1-phenylethanone

2-azido-2-(2-methoxyphenyl)-1-phenylethanone