ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate

Base Information

• Chemical Name: ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate
• CAS No.: 82777-30-8
• Molecular Formula: C₆H₅O₃S*C₁₉H₂₅O₂S₂
• Molecular Weight: 506.708
• Mol file: 82777-30-8.mol

Synonyms:ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate

Chemical Property of ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate

There total 3 articles about ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromopropyl p-tolyl sulphone (5755-77-1) → ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate (82777-30-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / 0.12 M sodium ethoxide / ethanol / 1 h / 80 °C

2: 1) dichloromethane, 4 h; ether, 0 deg C; 2) chloroform, 12 h

With sodium ethanolate; In ethanol;

DOI:10.1039/P29820000579

Reference yield:

para-thiocresol (106-45-6) → ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate (82777-30-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / 0.12 M sodium ethoxide / ethanol / 1 h / 80 °C

2: 1) dichloromethane, 4 h; ether, 0 deg C; 2) chloroform, 12 h

With sodium ethanolate; In ethanol;

DOI:10.1039/P29820000579

Reference yield:

triethyloxonium fluoroborate (368-39-8) + potassium benzenesulfonate (934-55-4) + C17H20O2S2 (82777-28-4) → ethyl-(3-p-tolylsulphonylpropyl)-p-tolylsulphonium benzenesulphonate (82777-30-8)

Guidance literature:

Yield given. Multistep reaction; 1) dichloromethane, 4 h; ether, 0 deg C; 2) chloroform, 12 h;

DOI:10.1039/P29820000579

upstream raw materials:

triethyloxonium fluoroborate

potassium benzenesulfonate

C₁₇H₂₀O₂S₂

3-bromopropyl p-tolyl sulphone

Downstream raw materials:

ethyl p-tolyl sulfide

2-ethoxy-propyl p-tolyl sulphone