methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

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Chemical Name:methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate
CAS No.:265658-99-9
Molecular Formula:C₂₁H₂₅NO₆
Molecular Weight:387.433
Hs Code.:

Synonyms:methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

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Chemical Property of methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

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Technology Process of methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

There total 3 articles about methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 108-59-8
malonic acid dimethyl ester

: 265658-94-4
3-{N-benzyl[(E)-but-2-enyl]amino}-2-(methoxycarbonyl)acrolein

: 265658-99-9
methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

Guidance literature:: With pyridine; titanium tetrachloride; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/S0040-4020(00)00029-6

Reference yield:

: 64516-52-5
2-(methoxycarbonyl)malonaldehyde

: 265658-99-9
methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / tetrahydrofuran / 20 °C

2: 55 percent / TiCl₄; pyridine / tetrahydrofuran / 20 °C

With pyridine; titanium tetrachloride; In tetrahydrofuran; 1: Substitution / 2: Condensation;
DOI:10.1016/S0040-4020(00)00029-6

Reference yield:

: 107733-62-0
benzyl crotyl amine

: 265658-99-9
methyl 5-{N-benzyl[(E)-but-2-enyl]amino}-2,4-bis(methoxycarbonyl)penta-2,4-dienate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / tetrahydrofuran / 20 °C

2: 55 percent / TiCl₄; pyridine / tetrahydrofuran / 20 °C

With pyridine; titanium tetrachloride; In tetrahydrofuran; 1: Substitution / 2: Condensation;
DOI:10.1016/S0040-4020(00)00029-6