4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

Base Information

Chemical Name:4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate
CAS No.:93684-52-7
Molecular Formula:C₇H₇O₃S*C₂₁H₂₄NO
Molecular Weight:477.624
Hs Code.:

Synonyms:4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

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Chemical Property of 4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

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Technology Process of 4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

There total 3 articles about 4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 4873-09-0
allyl tosylate

: 93684-43-6
4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)oxazole

: 93684-52-7
4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

Guidance literature:: at 50 ℃; for 24h;
DOI:10.1021/ja00288a028

Reference yield:

: 1795-98-8,3182-95-4,5267-64-1,16088-07-6
rac-phenylalaninol

: 93684-52-7
4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / xylene / 16 h / Heating

2: 92 percent / 24 h / 50 °C

In xylene;
DOI:10.1021/ja00288a028

Reference yield:

: 501-52-0
3-Phenylpropionic acid

: 93684-52-7
4,5-dihydro-2-(2-phenylethyl)-4-(phenylmethyl)-3-(2-propenyl)oxazolinium 4-methylbenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / xylene / 16 h / Heating

2: 92 percent / 24 h / 50 °C

In xylene;
DOI:10.1021/ja00288a028