rac-phenylalaninol

Base Information

• Chemical Name: rac-phenylalaninol
• CAS No.: 1795-98-8
• Molecular Formula: C₉H₁₃NO
• Molecular Weight: 151.208

Synonyms:

Chemical Property of rac-phenylalaninol

Chemical Property:

Purity/Quality:

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Technology Process of rac-phenylalaninol

There total 24 articles about rac-phenylalaninol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Phenylalanine (150-30-1,25191-15-5,658-69-5,67675-33-6) → rac-phenylalaninol (1795-98-8,3182-95-4,5267-64-1,16088-07-6)

Guidance literature:

With sodium tetrahydroborate; iodine;

DOI:10.1002/cctc.202000597

Reference yield: 80.0%

ethyl 2-(hydroxyimino)-3-phenylpropanoate (6943-96-0,70564-52-2,70564-53-3) → rac-phenylalaninol (1795-98-8,3182-95-4,5267-64-1,16088-07-6)

Guidance literature:

With sodium tetrahydroborate; iodine; In tetrahydrofuran; for 4h; Heating;

DOI:10.1055/s-2003-41046

Reference yield: 77.0%

Phenylalanine (150-30-1,25191-15-5,658-69-5,67675-33-6) + dimethyl sulfide borane (13292-87-0) → rac-phenylalaninol (1795-98-8,3182-95-4,5267-64-1,16088-07-6)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; water;

upstream raw materials:

ethyl N-acetyl-DL-phenylalaninate

Z-β-ethoxycarbonyl-β-nitrostyrene

phenylalanine ethyl ester

acetic acid-(β-nitro-cinnamyl ester)

Downstream raw materials:

1-bromomethyl-2-phenyl-ethylamine

2-acetamido-3-phenylpropanol acetate

2-(2,4-dinitro-anilino)-3-phenyl-propan-1-ol

2-benzoylamino-1-benzoyloxy-3-phenyl-propane

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