(E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide

Base Information

• Chemical Name: (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide
• CAS No.: 1427059-39-9
• Molecular Formula: C₁₄H₂₀N₅*I
• Molecular Weight: 385.251

Synonyms:(E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide

Chemical Property of (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide

Chemical Property:

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Technology Process of (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide

There total 2 articles about (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(E)-N-(4-(diethylamino)benzylidene)-4H-1,2,4-triazol-4-amine (1159652-53-5) + methyl iodide (74-88-4) → (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide (1427059-39-9)

Guidance literature:

for 5h; Reflux; Inert atmosphere;

DOI:10.1021/jo302697q

Reference yield:

4-Diethylaminobenzaldehyde (120-21-8) → (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide (1427059-39-9)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / ethanol / 5 h / Reflux; Inert atmosphere

2: 5 h / Reflux; Inert atmosphere

With sulfuric acid; In ethanol;

DOI:10.1021/jo302697q

Reference yield: 68.0%

4-nitrophenyl azide (1516-60-5) + (E)-4-((4-(diethylamino)benzylidene)amino)-1-methyl-4H-1,2,4-triazol-1-ium iodide (1427059-39-9) → N,N-diethyl-4-((E)-(((E)-1-methyl-5-((E)-(4-nitrophenyl)triaz-2-en-1-ylidene)-1,5-dihydro-4H-1,2,4-triazol-4-yl)imino)-methyl)aniline (1427059-20-8)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at -78 - 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/jo302697q

upstream raw materials:

4-Diethylaminobenzaldehyde

(E)-N-(4-(diethylamino)benzylidene)-4H-1,2,4-triazol-4-amine

methyl iodide

Downstream raw materials:

N,N-diethyl-4-((E)-(((E)-1-methyl-5-((E)-(4-nitrophenyl)triaz-2-en-1-ylidene)-1,5-dihydro-4H-1,2,4-triazol-4-yl)imino)-methyl)aniline

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