Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

Base Information

Chemical Name:Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester
CAS No.:195821-92-2
Molecular Formula:C₂₅H₂₉NO₅
Molecular Weight:423.509
Hs Code.:

Synonyms:Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

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Chemical Property of Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

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Technology Process of Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

There total 1 articles about Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 107941-22-0
2-bromo-1,4,5-trimethoxynaphthalene

: C₃₆H₄₈BN₃O₇

: 195821-92-2
Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; toluene; Heating;
DOI:10.1021/jo971123d

Reference yield:

: 195821-92-2
Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

: 195821-94-4
3-(2-Hydroxy-4-methyl-3-trimethylsilanyl-phenyl)-1,4,8-trimethoxy-naphthalene-2-carboxylic acid diethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) s-BuLi, TMEDA / 1.) THF, -98 deg C

2: 62 percent / LDA / tetrahydrofuran / Ambient temperature

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo971123d

Reference yield:

: 195821-92-2
Diethyl-carbamic acid 5-methyl-2-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl ester

: N,N-Diethyl-2-{[2-hydroxy-6-methyl-3-(1,4,5-trimethoxy-naphthalen-2-yl)-phenyl]-dimethyl-silanyl}-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) s-BuLi, TMEDA / 1.) THF, -98 deg C

2: 17 percent / LDA / tetrahydrofuran / Ambient temperature

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/jo971123d