C₁₁H₁₁BrO₅

Base Information

Chemical Name:C₁₁H₁₁BrO₅
CAS No.:1271777-58-2
Molecular Formula:C₁₁H₁₁BrO₅
Molecular Weight:303.109
Hs Code.:

C<sub>11</sub>H<sub>11</sub>BrO<sub>5</sub>

Synonyms:C₁₁H₁₁BrO₅

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Chemical Property of C₁₁H₁₁BrO₅

Chemical Property:

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Technology Process of C₁₁H₁₁BrO₅

There total 1 articles about C₁₁H₁₁BrO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1271773-53-5
C₁₅H₁₉BrO₅

: 1271777-58-2
C₁₁H₁₁BrO₅

Guidance literature:: C₁₅H₁₉BrO₅; With water; sodium hydroxide; In 1,4-dioxane; at 20 ℃; for 5h; Heating; Reflux;

With hydrogenchloride; In water; at 20 ℃;

Reference yield: 77.0%

: 64-17-5
ethanol

: 1271777-58-2
C₁₁H₁₁BrO₅

: 1271773-56-8
C₁₃H₁₅BrO₅

Guidance literature:: C₁₁H₁₁BrO₅; With trifluoroacetic anhydride; at 0 - 20 ℃; Inert atmosphere;

ethanol; at 20 ℃;

Reference yield:

: 1271777-58-2
C₁₁H₁₁BrO₅

: C₂₄H₂₇NO₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: trifluoroacetic anhydride / 0 - 20 °C / Inert atmosphere

1.2: 20 °C

2.1: triethylamine / benzene / 20 °C / Inert atmosphere

2.2: 20 °C / Reflux; Inert atmosphere

3.1: dmap; triethylamine / dichloromethane / 4 h / 20 °C / Inert atmosphere

4.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene / 2 h / 90 °C / Inert atmosphere

With dmap; potassium carbonate; triethylamine; trifluoroacetic anhydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene; benzene;