1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

Base Information

Chemical Name:1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide
CAS No.:130091-15-5
Molecular Formula:C₂₄H₂₁N₅O₂S
Molecular Weight:443.529
Hs Code.:

Synonyms:1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

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Chemical Property of 1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

Chemical Property:

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Technology Process of 1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

There total 4 articles about 1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 103-72-0
phenyl isothiocyanate

: 130090-87-8
2-(4-benzyl-1-oxophthalazin-2(1H)-yl)acetohydrazide

: 130091-15-5
1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

Guidance literature:: In benzene; for 5h; Heating;

Reference yield:

: 132544-84-4
4-benzyl-1(2H)-oxophthalazin-2-acetic acid ethyl ester

: 130091-15-5
1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / N₂H₄*H₂O / ethanol / 4 h / Heating

2: 93 percent / benzene / 5 h / Heating

With hydrazine hydrate; In ethanol; benzene;

Reference yield:

: 32003-14-8
4-benzyl-2H-phthalazin-1-one

: 130091-15-5
1-((4-benzyl-1-oxo-1H-phthalazin-2-yl)acetyl)-4-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 5percent NaOH / ethanol / 1 h / Heating

2: 94 percent / N₂H₄*H₂O / ethanol / 4 h / Heating

3: 93 percent / benzene / 5 h / Heating

With sodium hydroxide; hydrazine hydrate; In ethanol; benzene;