2-(2-methoxyphenyl)propanoic acid ethyl ester

Base Information

Chemical Name:2-(2-methoxyphenyl)propanoic acid ethyl ester
CAS No.:128950-12-9
Molecular Formula:C₁₂H₁₆O₃
Molecular Weight:208.257
Hs Code.:

Synonyms:2-(2-methoxyphenyl)propanoic acid ethyl ester

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Chemical Property of 2-(2-methoxyphenyl)propanoic acid ethyl ester

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Technology Process of 2-(2-methoxyphenyl)propanoic acid ethyl ester

There total 3 articles about 2-(2-methoxyphenyl)propanoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 81616-76-4
2-(2-methoxyphenyl)propenoic acid ethyl ester

: 128950-12-9
2-(2-methoxyphenyl)propanoic acid ethyl ester

Guidance literature:: With palladium on activated charcoal; hydrogen; In methanol; at 20 ℃; for 4h; under 2327.23 Torr;
DOI:10.1002/hlca.201500062

Reference yield:

: 64-17-5
ethanol

: 81616-80-0,81616-81-1,91061-46-0,96687-71-7
(S)-2(2-methoxyphenyl)propionic acid

: 128950-12-9
2-(2-methoxyphenyl)propanoic acid ethyl ester

Guidance literature:: With sulfuric acid; at 0 ℃; for 7.08333h; Reflux; Inert atmosphere;
DOI:10.3390/molecules17067356

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 128950-12-9
2-(2-methoxyphenyl)propanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrafluoroboric acid diethyl ether / dichloromethane / Inert atmosphere; Schlenk technique

1.2: 12 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: 3,3-diphenyl-1-methylpyrrolidino[1,2-c]-1,3,2-oxazaborole; borane-THF / tetrahydrofuran / 0 °C / Inert atmosphere; Schlenk technique

3.1: palladium on activated charcoal; hydrogen / methanol / 4 h / 20 °C / 2327.23 Torr

With tetrafluoroboric acid diethyl ether; borane-THF; 3,3-diphenyl-1-methylpyrrolidino[1,2-c]-1,3,2-oxazaborole; palladium on activated charcoal; hydrogen; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/hlca.201500062