2-[3-(3-Methylphenyl)propyl]-1,3-dioxolane

Base Information

Chemical Name:2-[3-(3-Methylphenyl)propyl]-1,3-dioxolane
CAS No.:313058-68-3
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:
DSSTox Substance ID:DTXSID401266544

Synonyms:2-[3-(3-methylphenyl)propyl]-1,3-dioxolane;DTXSID401266544;313058-68-3

Suppliers and Price of 2-[3-(3-Methylphenyl)propyl]-1,3-dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[3-(3-Methylphenyl)propyl]-1,3-dioxolane

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:206.130679813
Heavy Atom Count:15
Complexity:175

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=CC=C1)CCCC2OCCO2

Technology Process of 2-[3-(3-Methylphenyl)propyl]-1,3-dioxolane

There total 1 articles about 2-[3-(3-Methylphenyl)propyl]-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1193-18-6
3-methylcyclohexen-2-one

: 120447-87-2
2-<3-(Phenylsulfonyl)propyl>-1,3-dioxolane

: 313058-68-3
2-(3-m-tolyl-propyl)-[1,3]dioxolane

Guidance literature:: 2-<3-(Phenylsulfonyl)propyl>-1,3-dioxolane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

3-methylcyclohexen-2-one; With benzoyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h;

With potassium tert-butylate; In tetrahydrofuran; hexane; for 3h; Heating;
DOI:10.1002/(SICI)1521-3773(19990802)38:15<2267::AID-ANIE2267>3.0.CO;2-3

Reference yield: 97.0%

: 313058-68-3
2-(3-m-tolyl-propyl)-[1,3]dioxolane

: 22156-45-2
4-(m-tolyl)butanoic acid

Guidance literature:: With Oxone; water; In tetrahydrofuran; at 0 - 20 ℃; for 12h;
DOI:10.1002/(SICI)1521-3773(19990802)38:15<2267::AID-ANIE2267>3.0.CO;2-3

Reference yield:

: 313058-68-3
2-(3-m-tolyl-propyl)-[1,3]dioxolane

: 51015-29-3
6-methyl-3,4-dihydronaphthalen-1(2H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / OXONE; H₂O / tetrahydrofuran / 12 h / 0 - 20 °C

2: 97 percent / TfOH / 2 h / 5 - 20 °C

With Oxone; trifluorormethanesulfonic acid; water; In tetrahydrofuran; 1: Hydrolysis / 2: Cyclization;
DOI:10.1002/(SICI)1521-3773(19990802)38:15<2267::AID-ANIE2267>3.0.CO;2-3