7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

Base Information

Chemical Name:7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester
CAS No.:151699-11-5
Molecular Formula:C₂₀H₂₁NO₂
Molecular Weight:307.392
Hs Code.:

Synonyms:7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

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Chemical Property of 7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

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Technology Process of 7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

There total 5 articles about 7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (Z)-2-Azido-3-[2-((1E,3E)-4-phenyl-buta-1,3-dienyl)-cyclohex-1-enyl]-acrylic acid methyl ester

: 151699-11-5
7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

Guidance literature:: In cyclohexane; at 80 ℃; for 0.666667h; Yield given;

Reference yield:

: 52378-69-5,58922-31-9,149298-72-6
diethyl cinnamylphosphonate

: 151699-11-5
7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran / Ambient temperature

2: 1.) t-BuLi / 1.) THF, -78 deg C, 2.) -78 deg C to r. t.

3: NaOMe / methanol / 0 deg C to r. t.

4: cyclohexane / 0.67 h / 80 °C

With tert.-butyl lithium; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; cyclohexane;

Reference yield:

: 38127-47-8
2-bromocyclohex-1-ene-1-carbaldehyde

: 151699-11-5
7a-((1E,3E)-4-Phenyl-buta-1,3-dienyl)-5,6,7,7a-tetrahydro-4H-indole-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran / Ambient temperature

2: 1.) t-BuLi / 1.) THF, -78 deg C, 2.) -78 deg C to r. t.

3: NaOMe / methanol / 0 deg C to r. t.

4: cyclohexane / 0.67 h / 80 °C

With tert.-butyl lithium; sodium methylate; sodium hydride; In tetrahydrofuran; methanol; cyclohexane;