N-allyl-2,2-diethoxy-1-phenylethylamine

Base Information

Chemical Name:N-allyl-2,2-diethoxy-1-phenylethylamine
CAS No.:157422-73-6
Molecular Formula:C₁₅H₂₃NO₂
Molecular Weight:249.353
Hs Code.:

Synonyms:N-allyl-2,2-diethoxy-1-phenylethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-2,2-diethoxy-1-phenylethylamine

Chemical Property:

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Technology Process of N-allyl-2,2-diethoxy-1-phenylethylamine

There total 1 articles about N-allyl-2,2-diethoxy-1-phenylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6175-45-7
2,2-diethoxyacetophenone

: 107-11-9,30551-89-4
1-amino-2-propene

: 157422-73-6
N-allyl-2,2-diethoxy-1-phenylethylamine

Guidance literature:: With 3 A molecular sieve; sodium cyanoborohydride; acetic acid; Yield given. Multistep reaction; 1.) ethanol, 1 h, 2.) ethanol, RT, 2 d;
DOI:10.1021/jm00001a014

Reference yield:

: 157422-73-6
N-allyl-2,2-diethoxy-1-phenylethylamine

: 2-(8-carboxy-1-oxo-3-phenyl-1,2-dihydropyrido<3,4-b>indol-2-yl)-N-(3,3,3-trifluoro-1-isopropyl-2-oxopropyl)acetamide

Guidance literature:: Multi-step reaction with 10 steps

1: triethylamine / CH₂Cl₂

2: conc. sulfuric acid / diethyl ether / 3 h

3: 1.) N-methylmorpholine N-oxide, osmium tetraoxide, 2.) sodium periodate / 1.) THF, H₂O, overnight, 2.) ethanol, H₂O, 2 h

4: sodium chlorite, sodium dihydrogen phosphate monohydrate / tetrahydrofuran; 2-methyl-propan-2-ol; various solvent(s); H₂O / 0.5 h

5: 1-hydroxybenzotriazole, triethylamine, 1-<3-(dimethylamino)propyl>-3-ethylcarbodimide / dimethylformamide

6: nitromethane, aluminum chloride / benzene / 1 h

7: sodium chlorite, sodium dihydrogen phosphate / 2-methyl-propan-2-ol; tetrahydrofuran; various solvent(s); H₂O / 0.5 h

8: 48 percent / methanol; diethyl ether

9: 1-<3-(dimethylamino)propyl>-3-ethylcarbodimide, dichloroacetic acid / dimethylsulfoxide; toluene / 2 h / Ambient temperature

10: 61 percent / lithium hydroxide monohydrate / tetrahydrofuran; H₂O / 1 h

With dichloro-acetic acid; lithium hydroxide; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; aluminium trichloride; sodium dihydrogen phosphate; nitromethane; sulfuric acid; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene;
DOI:10.1021/jm00001a014

Reference yield:

: 157422-73-6
N-allyl-2,2-diethoxy-1-phenylethylamine

: 1026864-34-5
2-<8-(methoxycarbonyl)-1-oxo-3-phenyl-1,2-dihydropyrido<3,4-b>indol-2-yl>-N-(3,3,3-trifluoro-2-hydroxy-1-isopropylpropyl)acetamide

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / CH₂Cl₂

2: conc. sulfuric acid / diethyl ether / 3 h

3: 1.) N-methylmorpholine N-oxide, osmium tetraoxide, 2.) sodium periodate / 1.) THF, H₂O, overnight, 2.) ethanol, H₂O, 2 h

4: sodium chlorite, sodium dihydrogen phosphate monohydrate / tetrahydrofuran; 2-methyl-propan-2-ol; various solvent(s); H₂O / 0.5 h

5: 1-hydroxybenzotriazole, triethylamine, 1-<3-(dimethylamino)propyl>-3-ethylcarbodimide / dimethylformamide

6: nitromethane, aluminum chloride / benzene / 1 h

7: sodium chlorite, sodium dihydrogen phosphate / 2-methyl-propan-2-ol; tetrahydrofuran; various solvent(s); H₂O / 0.5 h

8: 48 percent / methanol; diethyl ether

With sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; aluminium trichloride; sodium dihydrogen phosphate; nitromethane; sulfuric acid; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/jm00001a014