Li(C₄H₈O)4⁽¹⁺⁾*C₃₂H₂₄P₃(Ni(CO)3)2^(1-)=[Li(C₄H₈O)4][C₃₂H₂₄P₃(Ni(CO)3)2]

Base Information

• Chemical Name: Li(C₄H₈O)4⁽¹⁺⁾*C₃₂H₂₄P₃(Ni(CO)3)2^(1-)=[Li(C₄H₈O)4][C₃₂H₂₄P₃(Ni(CO)3)2]
• CAS No.: 235754-72-0
• Molecular Formula: C₁₆H₃₂LiO₄*C₃₈H₂₄Ni₂O₆P₃
• Molecular Weight: 1082.27

Synonyms:Li(C₄H₈O)4⁽¹⁺⁾*C₃₂H₂₄P₃(Ni(CO)3)2^(1-)=[Li(C₄H₈O)4][C₃₂H₂₄P₃(Ni(CO)3)2]

Chemical Property of Li(C₄H₈O)4⁽¹⁺⁾*C₃₂H₂₄P₃(Ni(CO)3)2^(1-)=[Li(C₄H₈O)4][C₃₂H₂₄P₃(Ni(CO)3)2]

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Technology Process of Li(C₄H₈O)4⁽¹⁺⁾*C₃₂H₂₄P₃(Ni(CO)3)2^(1-)=[Li(C₄H₈O)4][C₃₂H₂₄P₃(Ni(CO)3)2]

There total 1 articles about Li(C₄H₈O)4⁽¹⁺⁾*C₃₂H₂₄P₃(Ni(CO)3)2^(1-)=[Li(C₄H₈O)4][C₃₂H₂₄P₃(Ni(CO)3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

Li(1+)*C32H24P3(1-)*99C4H8O=Li[C32H24P3]*99C4H8O + tetracarbonyl nickel (13463-39-3,71564-36-8) → Li(C4H8O)4(1+)*C32H24P3(Ni(CO)3)2(1-)=[Li(C4H8O)4][C32H24P3(Ni(CO)3)2] (235754-72-0)

Guidance literature:

In tetrahydrofuran; byproducts: CO; addn. of soln. of Li compound to soln. of excess Ni(CO)4, stirring (2 h); concn., addn. (Et2O), filtration, pptn. (2°C, several weeks), recrystn. (THF);

DOI:10.1002/(sici)1099-0682(199907)1999:7<1169::aid-ejic1169>3.0.co;2-q

upstream raw materials:

tetracarbonyl nickel

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