1,4-Cyclohexanedione,1,4-dioxime

Base Information

• Chemical Name: 1,4-Cyclohexanedione,1,4-dioxime
• CAS No.: 10220-83-4
• Molecular Formula: C₆H₁₀N₂O₂
• Molecular Weight: 142.158
• Mol file: 10220-83-4.mol

Synonyms:1,4-Cyclohexanedione,dioxime (6CI,7CI,8CI,9CI); 1,4-Bis(hydroxyimino)cyclohexane;1,4-Cyclohexanedioxime; NSC 145140; p-Cyclohexanedione dioxime

Chemical Property of 1,4-Cyclohexanedione,1,4-dioxime

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,4-Cyclohexanedione,1,4-dioxime

There total 5 articles about 1,4-Cyclohexanedione,1,4-dioxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1,4-Cyclohexanedione (637-88-7) → 1,4-cyclohexanedioxime (6133-84-2,6212-72-2,10220-83-4)

Guidance literature:

1,4-Cyclohexanedione; With hydroxylamine hydrochloride; In water; at 0 - 20 ℃; for 0.5h;

With potassium carbonate; In water;

DOI:10.1002/cplu.201300014

Reference yield: 78.0%

1,4-Cyclohexanedione (637-88-7) → cyclohexane-1,4-dione dioxime (10220-83-4,6212-72-2,6133-84-2)

Guidance literature:

With sodium hydroxide; ethanol; NH₂O*HCl; for 0.5h;

DOI:10.1016/j.tetlet.2004.03.084

Reference yield:

trans-1,4-Dinitroso-1,4-dichlorcyclohexan (18993-06-1) → cyclohexane-1,4-dione dioxime (10220-83-4,6212-72-2,6133-84-2)

Guidance literature:

With ethanol; hydrazine hydrate;

upstream raw materials:

trans-1,4-Dinitroso-1,4-dichlorcyclohexan

1,4-Cyclohexanedione

ethanol

1,4-dichloro-1,4-dinitro-cyclohexane

Downstream raw materials:

1,4-dibromo-1,4-dinitroso-cyclohexane

cyclohexane-1,4-dione-bis-[O-(toluene-4-sulfonyl)-oxime ]

1.4-Bis-dimethylamino-cyclohexan

N-(4-formamidocyclohexyl)formamide