5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

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Chemical Name:5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine
CAS No.:1383687-94-2
Molecular Formula:C₂₄H₃₄N₂₀O₁₀
Molecular Weight:762.662
Hs Code.:

Synonyms:5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

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Chemical Property of 5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

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Technology Process of 5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

There total 5 articles about 5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88192-19-2
3-azidopropylamine

: 1383687-47-5
5,6-[carbonylbis(oxy)]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

: 1383687-94-2
5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

Guidance literature:: 3-azidopropylamine; 5,6-[carbonylbis(oxy)]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine; In dichloromethane; at 20 ℃; for 2h;

With 4-Nitrophenyl chloroformate; In dichloromethane; at 20 ℃;

3-azidopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c2ob07065k

Reference yield:

: 182554-04-7
1,3,2′,6′-tetraazido-6,3′,4′-tri-O-acetylneamine

: 1383687-94-2
5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / tetrahydrofuran / 1 h / 20 °C

2.1: pyridine / dichloromethane / -78 °C / Inert atmosphere

3.1: dichloromethane / 2 h / 20 °C

3.2: 20 °C

3.3: 2 h / 20 °C

With pyridine; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob07065k

Reference yield:

: 671809-10-2
1,3,2′,6′-tetraazidoneamine

: 1383687-94-2
5,6-di-[[(3-azidopropylamino)carbonyl]oxy]-3',4'-di-O-acetyl-1,3,2',6'-tetraazidoneamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

2.1: sodium hydroxide / tetrahydrofuran / 1 h / 20 °C

3.1: pyridine / dichloromethane / -78 °C / Inert atmosphere

4.1: dichloromethane / 2 h / 20 °C

4.2: 20 °C

4.3: 2 h / 20 °C

With pyridine; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob07065k