(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

Base Information

Chemical Name:(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide
CAS No.:153109-51-4
Molecular Formula:C₂₂H₃₆INO₃Si
Molecular Weight:517.523
Hs Code.:

Synonyms:(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

Suppliers and Price of (Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

There total 4 articles about (Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 139115-75-6
2-iodo-4-methoxy-N-methylaniline

: (Z)-1-Benzotriazol-1-yl-2-methyl-4-triisopropylsilanyloxy-but-2-en-1-one

: 153109-51-4
(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

Guidance literature:: at 60 ℃; for 4h;
DOI:10.1021/ja980788+

Reference yield: 55.0%

: 139115-75-6
2-iodo-4-methoxy-N-methylaniline

: 153109-50-3
(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid

: 153109-51-4
(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; Heating;
DOI:10.1021/ja980788+

Reference yield:

: 153109-50-3
(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid

: 153109-51-4
(Z)-2-Methyl-4-triisopropylsilanyloxy-but-2-enoic acid (2-iodo-4-methoxy-phenyl)-methyl-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 80 percent / 4 h / 60 °C

With triethylamine; In dichloromethane;
DOI:10.1021/ja980788+