3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Base Information

Chemical Name:3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one
CAS No.:1276544-28-5
Molecular Formula:C₂₀H₁₈F₂N₄OS
Molecular Weight:400.452
Hs Code.:

Synonyms:3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Suppliers and Price of 3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

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Technology Process of 3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

There total 5 articles about 3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1216065-47-2
C₁₇H₁₅F₂NO

: 79-19-6
thiosemicarbazide

: 105-39-5
chloroacetic acid ethyl ester

: 1276544-28-5
3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Guidance literature:: With silica gel supported sodium hydrogen sulphate; for 0.0666667h; Microwave irradiation;
DOI:10.3109/14756361003691878

Reference yield: 78.0%

: 1286795-50-3
C₁₈H₁₈F₂N₄S

: 105-39-5
chloroacetic acid ethyl ester

: 1276544-28-5
3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Guidance literature:: With sodium acetate; In ethanol; for 4h; Reflux;
DOI:10.1016/j.bmcl.2009.11.074

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 1276544-28-5
3-(2,6-bis(4-fluorophenyl)piperidin-4-ylideneamino)-2-thioxoimidazolidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / Heating

2: ethanol / 2 h / Reflux

3: sodium acetate / ethanol / 4 h / Reflux

With ammonium acetate; sodium acetate; In ethanol;
DOI:10.3109/14756361003691878