C₁₇H₂₃FN₂O₃

Base Information

Chemical Name:C₁₇H₂₃FN₂O₃
CAS No.:1611481-00-5
Molecular Formula:C₁₇H₂₃FN₂O₃
Molecular Weight:322.38
Hs Code.:

C<sub>17</sub>H<sub>23</sub>FN<sub>2</sub>O<sub>3</sub>

Synonyms:C₁₇H₂₃FN₂O₃

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Chemical Property of C₁₇H₂₃FN₂O₃

Chemical Property:

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Technology Process of C₁₇H₂₃FN₂O₃

There total 14 articles about C₁₇H₂₃FN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40216-83-9
L-4-hydroxyproline methyl ester hydrochloride

: 1611481-00-5
C₁₇H₂₃FN₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1: triethylamine / dichloromethane / 8 h / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

3: sodium azide / N,N-dimethyl-formamide / 8 h / 65 °C / Inert atmosphere

4: lithium aluminium tetrahydride / tetrahydrofuran / 3.5 h / 0 - 20 °C / Inert atmosphere

5: 1,4-dioxane / 20 h / 20 °C / Inert atmosphere

6: diethylamino-sulfur trifluoride / tetrahydrofuran / 13 h / 0 - 20 °C / Inert atmosphere

7: palladium 10% on activated carbon; formic acid; piperidine / tetrahydrofuran / Microwave irradiation

8: triethylamine / dichloromethane / 9 h / 20 °C / Inert atmosphere

With piperidine; lithium aluminium tetrahydride; formic acid; sodium azide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201302423

Reference yield:

: 1405128-38-2,1593969-81-3
tert-butyl ((3S,5R)-5-fluoropiperidin-3-yl)carbamate

: 98-88-4
benzoyl chloride

: 1611481-00-5
C₁₇H₂₃FN₂O₃

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 9h; Inert atmosphere;
DOI:10.1002/chem.201302423

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1611481-00-5
C₁₇H₂₃FN₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: 1,4-dioxane / 14 h / 20 °C / Inert atmosphere

2: diethylamino-sulfur trifluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

3: hydrogenchloride / water; ethanol / 1 h / 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 9 h / 20 °C / Inert atmosphere

With hydrogenchloride; diethylamino-sulfur trifluoride; triethylamine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1002/chem.201302423