2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether

Base Information

• Chemical Name: 2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether
• CAS No.: 1015098-70-0
• Molecular Formula: C₂₅H₂₂O
• Molecular Weight: 338.449
• Mol file: 1015098-70-0.mol

Synonyms:2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether

Chemical Property of 2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether

Chemical Property:

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Technology Process of 2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether

There total 1 articles about 2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methylene-4-phenylpent-4-en-1-ol (1015098-94-8) + 3-(α-Naphthyl)propargyl bromide (352035-98-4) → 2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether (1015098-70-0)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ja0762083

Reference yield:

2-methylene-4-phenylpent-4-enyl 3-(1-naphthyl)prop-2-ynyl ether (1015098-70-0) → (Z)-4-(1-naphthylmethylene)-7-phenyl-2-oxaspiro[4.4]non-6-ene + C25H22O

Guidance literature:

bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; 2,2’-bis(diphenylphosphino)-1,1’-binaphthyl; In 1,2-dichloro-ethane; at 20 ℃; for 24h; Title compound not separated from byproducts.;

DOI:10.1021/ja0762083

upstream raw materials:

2-methylene-4-phenylpent-4-en-1-ol

3-(α-Naphthyl)propargyl bromide