3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime

Base Information

• Chemical Name: 3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime
• CAS No.: 121511-07-7
• Molecular Formula: C₁₇H₁₇NO
• Molecular Weight: 251.328
• Mol file: 121511-07-7.mol

Synonyms:3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime

Chemical Property of 3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime

There total 1 articles about 3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-p-methylphenyl-1-tetralone (38425-35-3) → 3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime (121511-07-7)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 0.25h; Heating;

Reference yield:

3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime (121511-07-7) → N-(3-p-Tolyl-naphthalen-1-yl)-acetamide

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) acetic anhydride, 2.) HCl gas, 3.) NH₃ / 1.) acetic acid, 100 deg C, 10 min, 2.) 100 deg C, 1 h, 3.) H₂O

2: pyridine / 1 h / Heating

With hydrogenchloride; ammonia; acetic anhydride; In pyridine;

Reference yield:

3-p-Tolyl-3,4-dihydro-2H-naphthalen-1-one oxime (121511-07-7) → 3-p-tolylnaphthalen-1-amine (121511-11-3)

Guidance literature:

With hydrogenchloride; ammonia; acetic anhydride; Multistep reaction; 1.) acetic acid, 100 deg C, 10 min, 2.) 100 deg C, 1 h, 3.) H₂O;

upstream raw materials:

3-p-methylphenyl-1-tetralone

Downstream raw materials:

3-p-tolylnaphthalen-1-amine