C₂₃H₂₀BrNO₅

Base Information

Chemical Name:C₂₃H₂₀BrNO₅
CAS No.:1359015-51-2
Molecular Formula:C₂₃H₂₀BrNO₅
Molecular Weight:470.32
Hs Code.:

C<sub>23</sub>H<sub>20</sub>BrNO<sub>5</sub>

Synonyms:C₂₃H₂₀BrNO₅

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Chemical Property of C₂₃H₂₀BrNO₅

Chemical Property:

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Technology Process of C₂₃H₂₀BrNO₅

There total 4 articles about C₂₃H₂₀BrNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1337958-87-8
dimethyl 2,5-dibromoisophthalate

: 1207-92-7
2-methoxy-N-phenylaniline

: 1359015-51-2
C₂₃H₂₀BrNO₅

Guidance literature:: With copper(l) iodide; copper; potassium carbonate; In dibutyl ether; at 150 ℃; for 60h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo202623u

Reference yield:

: 379711-35-0
2,5-dibromoisophthalic acid

: 1359015-51-2
C₂₃H₂₀BrNO₅

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 18 h / Reflux

2: copper(l) iodide; copper; potassium carbonate / dibutyl ether / 60 h / 150 °C / Inert atmosphere

With copper(l) iodide; sulfuric acid; copper; potassium carbonate; In dibutyl ether;
DOI:10.1021/jo202623u

Reference yield:

: 24596-19-8
4-bromo-2,6-dimethylphenylamine

: 1359015-51-2
C₂₃H₂₀BrNO₅

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; hydrogen bromide; copper(I) bromide; sodium nitrite

2: potassium permanganate / water; tert-butyl alcohol / 19 h / Reflux

3: sulfuric acid / 18 h / Reflux

4: copper(l) iodide; copper; potassium carbonate / dibutyl ether / 60 h / 150 °C / Inert atmosphere

With potassium permanganate; copper(l) iodide; sulfuric acid; hydrogen bromide; copper; potassium carbonate; copper(I) bromide; sodium nitrite; In dibutyl ether; water; tert-butyl alcohol; 1: Sandmeyer reaction;
DOI:10.1021/jo202623u