(E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

Base Information

Chemical Name:(E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one
CAS No.:1616108-79-2
Molecular Formula:C₂₃H₂₂N₂O₃S
Molecular Weight:406.505
Hs Code.:

Synonyms:(E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

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Chemical Property of (E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

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Technology Process of (E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

There total 3 articles about (E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 96-50-4
2-thiazolylamine

: 1616108-66-7
(E)-2-hydroxy-3-isopropyl-5-(3-(4-methoxyphenyl)-3-oxoprop-1-en-1-yl)benzaldehyde

: 1616108-79-2
(E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1016/j.ejmech.2014.05.029

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 1616108-79-2
(E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / 4 h / 120 °C

1.2: 2 h / 100 °C

2.1: hydrogenchloride / water; 1,4-dioxane / 80 - 90 °C

3.1: ethanol / 3 h / Reflux

With hydrogenchloride; trifluoroacetic acid; In 1,4-dioxane; ethanol; water; 1.1: |Duff Aldehyde Synthesis / 1.2: |Duff Aldehyde Synthesis;
DOI:10.1016/j.ejmech.2014.05.029

Reference yield:

: 99865-46-0
4-hydroxy-5-isopropylisophthalaldehyde

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1616108-79-2
(E)-3-(4-hydroxy-3-isopropyl-5-((E)-(thiazol-2-ylimino)methyl)phenyl)-1-(4methoxy phenyl)prop-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water; 1,4-dioxane / 80 - 90 °C

2: ethanol / 3 h / Reflux

With hydrogenchloride; In 1,4-dioxane; ethanol; water;
DOI:10.1016/j.ejmech.2014.05.029