tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate

Base Information

Chemical Name:tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate
CAS No.:1033130-00-5
Molecular Formula:C₃₉H₄₉NO₄Si
Molecular Weight:623.908
Hs Code.:

Synonyms:tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate

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Chemical Property of tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate

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Technology Process of tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate

There total 1 articles about tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1033129-97-3
(E)-tert-butyl 4-((tert-butyldiphenylsilyl)oxy)but-2-enoate

: 17480-69-2
(S)-N-benzyl-1-phenylethylamine

: 1033130-00-5
tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate

Guidance literature:: (S)-N-benzyl-1-phenylethylamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃;

(E)-tert-butyl 4-((tert-butyldiphenylsilyl)oxy)but-2-enoate; In tetrahydrofuran; hexane; at -78 ℃;

With (2R,8aS)-(+)-(camphorylsulfonyl)oxaziridine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h; optical yield given as %de;
DOI:10.1039/b801357h

Reference yield: 82.0%

: 1033130-00-5
tert-butyl (2S,3S,αS)-2-hydroxy-3-[N-benzyl-N-(α-methylbenzyl)amino]-4-tert-butyldiphenylsilyloxybutanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1033130-04-9
tert-butyl (2S,3S)-2-hydroxy-3-[N-(tert-butoxycarbonyl)amino]-4-tert-butyldiphenylsilyloxy-butanoate

Guidance literature:: With palladium hydroxide on carbon; hydrogen; In ethyl acetate; for 12h; under 3800.26 Torr; optical yield given as %de;
DOI:10.1039/b801357h