4-formylphenyl sulfamate

Base Information

Chemical Name:4-formylphenyl sulfamate
CAS No.:319014-98-7
Molecular Formula:C₇H₇NO₄S
Molecular Weight:201.203
Hs Code.:

Synonyms:4-formylphenyl sulfamate

Suppliers and Price of 4-formylphenyl sulfamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-formylphenyl sulfamate

Chemical Property:

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Technology Process of 4-formylphenyl sulfamate

There total 2 articles about 4-formylphenyl sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 319014-98-7
4-formylphenyl sulfamate

Guidance literature:: With sulphamoyl chloride; sodium hydride; In toluene;
DOI:10.1016/S0960-894X(01)00086-5

Reference yield:

: 108-95-2,27073-41-2
phenol

: 319014-98-7
4-formylphenyl sulfamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: AlCl₃ / CH₂Cl₂

2.1: NaH / dimethylformamide / 0 °C

2.2: aminosulfonyl chloride / toluene; dimethylformamide / 10 h

With aluminium trichloride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide; 1.1: Friedel-Crafts reaction;
DOI:10.1016/S0960-894X(01)00482-6

Reference yield:

: 319014-98-7
4-formylphenyl sulfamate

: 4-(N-phenylaminomethyl)phenyl sulfamate

Guidance literature:: With sodium bicarbonate; sodium borohydrid; sodium acetate; acetic acid; aniline; In methanol; ethanol; chloroform; water;