3,6-distyrylphenanthrene

Base Information

• Chemical Name: 3,6-distyrylphenanthrene
• CAS No.: 694502-83-5
• Molecular Formula: C₃₀H₂₂
• Molecular Weight: 382.505
• Mol file: 694502-83-5.mol

Synonyms:3,6-distyrylphenanthrene

Chemical Property of 3,6-distyrylphenanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,6-distyrylphenanthrene

There total 2 articles about 3,6-distyrylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3,6-dibromophenanthrene (174735-02-5) → 3,6-distyrylphenanthrene (694502-83-5)

Guidance literature:

With sodium acetate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); In N,N-dimethyl acetamide; at 140 ℃; for 48h;

DOI:10.1002/ejoc.200300470

Reference yield: 70.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 3,6-dibromophenanthrene (174735-02-5) → 3-bromo-6-styrylphenanthrene + 3,6-distyrylphenanthrene (694502-83-5)

Guidance literature:

With sodium acetate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II); In N,N-dimethyl acetamide; at 140 ℃; for 48h;

DOI:10.1002/ejoc.200300470

Reference yield: 90.0%

3,6-distyrylphenanthrene (694502-83-5) → heptahelicene (59177-52-5,20508-10-5,16914-68-4,40122-35-8)

Guidance literature:

With iodine; methyloxirane; In toluene; UV-irradiation;

DOI:10.1002/ejoc.200300470

upstream raw materials:

styrene

3,6-dibromophenanthrene

Downstream raw materials:

heptahelicene

Refernces