methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester

Base Information

• Chemical Name: methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester
• CAS No.: 389627-89-8
• Molecular Formula: C₁₆H₂₅NO₆S
• Molecular Weight: 359.444

Synonyms:methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester

Chemical Property of methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester

Chemical Property:

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Technology Process of methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester

There total 1 articles about methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[2-(2-hydroxy-ethoxy)-2-phenyl-ethyl]-carbamic acid tert-butyl ester (389627-88-7) + methanesulfonyl chloride (124-63-0) → methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester (389627-89-8)

Guidance literature:

With triethanolamine; nitrogen; In tetrahydrofuran; chloroform;

Reference yield: 85.0%

methanesulfonic acid 2-(2-tert-butoxycarbonylamino-1-phenyl-ethoxy) ethyl ester (389627-89-8) → [2-(2-iodo-ethoxy)-2-phenyl-ethyl]-carbamic acid tert-butyl ester (389627-90-1)

Guidance literature:

With sodium iodide; nitrogen; In acetone;

upstream raw materials:

[2-(2-hydroxy-ethoxy)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

methanesulfonyl chloride

Downstream raw materials:

[2-(2-iodo-ethoxy)-2-phenyl-ethyl]-carbamic acid tert-butyl ester

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