{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

Base Information

Chemical Name:{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester
CAS No.:197021-55-9
Molecular Formula:C₃₀H₃₉N₂O₆PSi
Molecular Weight:582.709
Hs Code.:

{2-[3-(<i>tert</i>-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2<i>H</i>-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

Synonyms:{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

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Chemical Property of {2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

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Technology Process of {2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

There total 6 articles about {2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 107-18-6
allyl alcohol

: 197021-53-7
{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid

: 197021-55-9
{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;
DOI:10.1055/s-2001-12328

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 197021-55-9
{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / imidazole / dimethylformamide / 20 °C

2: 71 percent / Me₃SiCl; EtOH / CHCl₃ / 20 °C

3: 98 percent / Et₃N / aq. ethanol / 20 °C

4: 73 percent / DCC; DMAP / tetrahydrofuran / 20 °C

With 1H-imidazole; dmap; chloro-trimethyl-silane; ethanol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-2001-12328

Reference yield:

: 197021-51-5
(1,1-Diethoxy-ethyl)-{2-[(2R,3S,5R)-3-hydroxy-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid ethyl ester

: 197021-55-9
{2-[3-(tert-butyl-diphenyl-silanyloxy)-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-2-yl]-ethyl}-phosphinic acid allyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / imidazole / dimethylformamide / 20 °C

2: 71 percent / Me₃SiCl; EtOH / CHCl₃ / 20 °C

3: 98 percent / Et₃N / aq. ethanol / 20 °C

4: 73 percent / DCC; DMAP / tetrahydrofuran / 20 °C

With 1H-imidazole; dmap; chloro-trimethyl-silane; ethanol; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-2001-12328