(2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

Base Information

Chemical Name:(2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate
CAS No.:1009301-30-7
Molecular Formula:C₃₂H₃₇N₃O₄S
Molecular Weight:559.729
Hs Code.:

Synonyms:(2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

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Technology Process of (2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

There total 2 articles about (2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1202021-27-9
(2S)-methyl 2-{[(S)-2-(tert-butoxycarbonylamino)-3-(tritylthio)propanamido]-2-butenamido}-3-methylbutanoate

: 1009301-30-7
(2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/chem.200901552

Reference yield:

: 1009301-19-2
C₃₆H₄₁N₃O₆S

: 1009301-30-7
(2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

Guidance literature:: With tri-n-butyl-tin hydride; acetic acid; bis-triphenylphosphine-palladium(II) chloride; In dichloromethane; for 3h;
DOI:10.1021/ol702957z

Reference yield: 81.0%

: 1009301-30-7
(2S)-methyl 2-{(Z)-2-[(S)-2-amino-3-(tritylthio)propanamido]but-2-enamido}-3-methylbutanoate

: 1202021-21-3
(R)-2-[(S,E)-3-(4-methoxybenzyloxy)-7-(tritylthio)hept-4-enamido]-3-methylbutanoic acid

: 1202021-29-1
(5E,7S,11R,14S,17E,20S)-methyl 17-ethylidene-11,20-diisopropyl-7-(4-methoxybenzyloxy)-9,12,15,18-tetraoxo-1,1,1-triphenyl-14-(tritylthiomethyl)-2-thia-10,13,16,19-tetraazahenicos-5-en-21-oate

Guidance literature:: With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at -30 ℃; Inert atmosphere;
DOI:10.1002/chem.200901552