(2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

Base Information

Chemical Name:(2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide
CAS No.:141080-16-2
Molecular Formula:C₃₅H₄₁NO₃SSi
Molecular Weight:583.867
Hs Code.:

Synonyms:(2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

Suppliers and Price of (2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

Chemical Property:

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Technology Process of (2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

There total 2 articles about (2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 141080-20-8,141195-56-4
(2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylsulfinylmethyl)butanamide

: 141080-16-2
(2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

: 137528-09-7
(3S,4S)-3-<(R)-1-<(tert-butyldiphenylsilyl)oxy>ethyl>-1-(p-methoxybenzyl)-4-(phenylthio)azetidin-2-one

: 137623-87-1
(3S,4R)-3-<(R)-1-<(tert-butyldiphenylsilyl)oxy>ethyl>-1-(p-methoxybenzyl)-4-(phenylthio)azetidin-2-one

Guidance literature:: With ketene t-butyldimethylsilyl methyl acetal; zinc(II) iodide; In acetonitrile; at 70 ℃; for 8h; Yield given. Title compound not separated from byproducts;
DOI:10.1248/cpb.40.12

Reference yield:

: 130164-39-5,130164-40-8
ethyl (3R)-3-<(tert-butyldiphenylsilyl)oxy>-2-(phenylthiomethyl)butanoate

: 2393-23-9
4-methoxy-benzylamine

: 141080-16-2
(2S,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

: 141080-17-3
(2R,3R)-3-<(tert-butyldiphenylsilyl)oxy>-N-(p-methoxybenzyl)-2-(phenylthiomethyl)butanamide

Guidance literature:: With trimethylaluminum; Yield given. Multistep reaction. Yields of byproduct given; 1.) hexane, benzene, from 0 deg C to RT, 1 h, 2.) hexane, benzene, reflux, 3 d;
DOI:10.1248/cpb.40.12