(S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride

Base Information

• Chemical Name: (S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride
• CAS No.: 878649-34-4
• Molecular Formula: C₁₈H₂₈FN₃O₄S*ClH
• Molecular Weight: 437.963

Synonyms:(S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride

Chemical Property of (S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride

Chemical Property:

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Technology Process of (S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride

There total 1 articles about (S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{(S)-1-[3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-ylcarbamoyl]-3-methyl-butyl}-carbamic acid-tert-butyl ester (878649-33-3) → (S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride (878649-34-4)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 4h;

Reference yield:

benzothiophene-2-carboxylic acid chloride (39827-11-7) + (S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride (878649-34-4) → (S)-2-(2-benzo[b]thiophene-2-carboxylic acid)-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide (878649-35-5)

Guidance literature:

(S)-2-amino-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide hydrochloride; With carbonate-polystyrene resin; In methanol; for 2h; Polystyrene

benzothiophene-2-carboxylic acid chloride; With morpholinemethyl polystyrene resin; In 1,2-dichloro-ethane;

With trisamine polystyrene; In 1,2-dichloro-ethane; for 1.5h;

upstream raw materials:

{(S)-1-[3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-ylcarbamoyl]-3-methyl-butyl}-carbamic acid-tert-butyl ester

Downstream raw materials:

(S)-2-(2-benzo[b]thiophene-2-carboxylic acid)-4-methyl-pentanoic acid [3-hydroxy-1-(4-fluorobenzenesulfonyl)-azepan-4-yl]-amide

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