1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Base Information

Chemical Name:1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
CAS No.:1180009-36-2
Molecular Formula:C₁₅H₁₁F₉N₂O₄S
Molecular Weight:486.315
Hs Code.:

Synonyms:1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Chemical Property of 1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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MSDS Files:: SDS file from LookChem

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Technology Process of 1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

There total 1 articles about 1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1180009-32-8
1-acetyl-5-phenylpyrazolidin-3-one

: 36913-91-4
nonaflyl anhydride

: 1180009-36-2
1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Guidance literature:: With pyridine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo9011859

Reference yield: 97.0%

: 1180009-36-2
1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 28611-39-4
4-(dimethylamino)benzene-boronic acid

: 313671-16-8
4-(1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl)-N,N-dimethylaniline

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In ethanol; water; toluene; at 120 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jo9011859

Reference yield: 96.0%

: 6165-69-1
Thien-3-ylboronic acid

: 1180009-36-2
1-acetyl-5-phenyl-4,5-dihydro-1H-pyrazol-3-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 1180009-55-5
1-acetyl-5-phenyl-3-(3-thienyl)-4,5-dihydro-1H-pyrazole

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In ethanol; water; toluene; at 120 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jo9011859