(R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

Base Information

Chemical Name:(R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane
CAS No.:216099-54-6
Molecular Formula:C₁₅H₁₈O₃
Molecular Weight:246.306
Hs Code.:

Synonyms:(R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

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Technology Process of (R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

There total 5 articles about (R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1-benzoyloxy-1-cyclooctene

: 216099-54-6
(R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

Guidance literature:: With (5S,8R,9R)-2,2-dimethyl-10-oxo-1,3,6-trioxaspiro[4.5]decane-8,9-diyl diacetate; Oxone; ethylenediaminetetraacetic acid; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; In Dimethoxymethane; water; acetonitrile; at 0 ℃; for 8h; pH=7.0; optical yield given as %ee; aq. phosphate buffer;
DOI:10.1021/jo900330n

Reference yield: 32.0%

: 254762-99-7
1-(benzoyloxy)-1,2-epoxycyclooctane

: 216099-54-6
(R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

: (S)-2-benzoyloxy-4,4-dimethylcyclooctanone

: (R)-2-benzoyloxy-4,4-dimethylcyclooctanone

Guidance literature:: With [(R)-BINOL]2-Ti(OiPr)4; In diethyl ether; at 0 ℃; for 68.5h;
DOI:10.1021/jo0108515

Reference yield:

: 1-benzoyloxy-1-cyclooctene

: (S,S)-1-benzoyloxy-1,2-epoxycyclooctane

: 216099-54-6
(R,R)-1-(benzoyloxy)-1,2-epoxycyclooctane

Guidance literature:: With borax; Oxone; fructose derived ketone; tetra(n-butyl)ammonium hydrogensulfate; edetate disodium; potassium carbonate; In water; acetonitrile; at 0 ℃; for 1.5h; Yield given; Yields of byproduct given;
DOI:10.1016/S0040-4039(98)01711-0