(2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

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Chemical Name:(2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol
CAS No.:192047-43-1
Molecular Formula:C₃₀H₄₆O₄S₂Si
Molecular Weight:562.91
Hs Code.:

Synonyms:(2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

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Chemical Property of (2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

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Technology Process of (2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

There total 8 articles about (2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 95452-06-5
tert-butyl(1,3-dithian-2-yl)dimethylsilane

: 14618-80-5
(R)-benzyl glycidol

: 192047-43-1
(2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

Guidance literature:: tert-butyl(1,3-dithian-2-yl)dimethylsilane; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.0833333h;

(R)-benzyl glycidol; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; pentane; at -78 - -45 ℃; for 0.5h;
DOI:10.1021/ja0376238

Reference yield: 80.0%

: 14618-80-5
(R)-benzyl glycidol

: 192047-48-6
(1R)-(1-benzyloxymethyl-2-[1,3]dithian-2-yl-ethoxy)-tert-butyl-dimethyl-silane

: 192047-43-1
(2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

Guidance literature:: (1R)-(1-benzyloxymethyl-2-[1,3]dithian-2-yl-ethoxy)-tert-butyl-dimethyl-silane; With n-butyllithium; sodium t-butanolate; at -78 ℃; for 1h;

(R)-benzyl glycidol; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Further stages.;
DOI:10.1021/jo010873r

Reference yield: 29.0%

: 95452-06-5
tert-butyl(1,3-dithian-2-yl)dimethylsilane

: 14618-80-5
(R)-benzyl glycidol

: 195257-60-4
(2S)-2-[2-(p-methoxybenzyloxy)ethyl]oxirane

: 192047-43-1
(2R)-1-benzyloxy-3-{2-[(2R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-propan-2-ol

: (S)-1-{2-[(R)-3-Benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-propyl]-[1,3]dithian-2-yl}-4-(4-methoxy-benzyloxy)-butan-2-ol

: (S)-1-{2-[(S)-2-(tert-Butyl-dimethyl-silanyloxy)-4-(4-methoxy-benzyloxy)-butyl]-[1,3]dithian-2-yl}-4-(4-methoxy-benzyloxy)-butan-2-ol

Guidance literature:: tert-butyl(1,3-dithian-2-yl)dimethylsilane; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.0833333h;

(R)-benzyl glycidol; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; pentane; at -78 ℃; for 1h;

(2S)-2-[2-(p-methoxybenzyloxy)ethyl]oxirane; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 1h;
DOI:10.1021/ja0376238