O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate

Base Information

Chemical Name:O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate
CAS No.:1235996-03-8
Molecular Formula:C₂₇H₄₀O₅S₂
Molecular Weight:508.744
Hs Code.:

Synonyms:O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate

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Chemical Property of O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate

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Technology Process of O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate

There total 1 articles about O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1235996-06-1
C₂₅H₃₈O₅

: 74-88-4
methyl iodide

: 1235996-03-8
O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate

Guidance literature:: C₂₅H₃₈O₅; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; mineral oil; at 50 ℃; for 2h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 50 ℃; for 5h; Inert atmosphere;
DOI:10.1055/s-0029-1218732

Reference yield: 89.0%

: 1235996-03-8
O-{(1R,5R,6R)-6-[2,6-bis(methoxymethoxy)-4-pentylphenyl]-5-isopropenyl-2-methylcyclohex-2-en-1-yl} S-methyl dithiocarbonate

: 1235996-04-9
2-[(1R,6R)-6-isopropenyl-3-methylcyclohex-3-en-1-yl]-1,3-bis(methoxymethoxy)-5-pentylbenzene

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 20 ℃; Inert atmosphere; Heating;
DOI:10.1055/s-0029-1218732