methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

Base Information

Chemical Name:methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate
CAS No.:1085709-12-1
Molecular Formula:C₂₀H₁₆N₂O₄
Molecular Weight:348.358
Hs Code.:

Synonyms:methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

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Chemical Property of methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

Chemical Property:

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Technology Process of methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

There total 3 articles about methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1085709-16-5
methyl 1-(4-hydroxy-3-methoxyphenyl)tetrahydro-β-carboline-3-carboxylate

: 1085709-12-1
methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: With sulfur; In 5,5-dimethyl-1,3-cyclohexadiene; for 24h; Reflux;
DOI:10.1016/j.ejmech.2019.111919

Reference yield:

: 1085709-24-5
1-(4-hydroxy-3-methoxyphenyl)tetrahydro-β-carboline-3-carboxylic acid

: 1085709-12-1
methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: acetic acid; selenium(IV) oxide / 1 h / Inert atmosphere; Reflux

With selenium(IV) oxide; thionyl chloride; acetic acid;
DOI:10.1039/c4nj00262h

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1085709-12-1
methyl 1-(4-hydroxy-3-methoxyphenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid

2: thionyl chloride

3: acetic acid; selenium(IV) oxide / 1 h / Inert atmosphere; Reflux

With selenium(IV) oxide; thionyl chloride; acetic acid;
DOI:10.1039/c4nj00262h