3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

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Chemical Name:3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose
CAS No.:866454-16-2
Molecular Formula:C₁₈H₂₁NO₄S
Molecular Weight:347.435
Hs Code.:

Synonyms:3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

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Chemical Property of 3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

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Technology Process of 3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

There total 4 articles about 3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 866429-20-1
5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

: 100-39-0
benzyl bromide

: 866454-16-2
3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/jo051012b

Reference yield:

: 866429-13-2
5-deoxy-1,2-O-isopropylidene-α-L-erythro-pentofuran-3-ulose

: 866454-16-2
3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / CH₂Cl₂

1.2: 40 percent / CH₂Cl₂

2.1: 95 percent / sodium hydride / dimethylformamide; various solvent(s) / 4 h / 20 °C

With n-butyllithium; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo051012b

Reference yield:

: 852310-59-9
2,2,5-trimethyl-(3aS,5S,6R,6aS)-perhydrofurol[2,3-d][1,3]dioxol-6-ol

: 866454-16-2
3-O-benzyl-5-deoxy-1,2-O-isopropylidene-3-C-(thiazol-2-yl)-α-L-ribofuranose

Guidance literature:: Multi-step reaction with 3 steps

1.1: 74 percent / pyridinium dichromate; acetic anhydride / CH₂Cl₂ / 2 h / Heating

2.1: BuLi / CH₂Cl₂

2.2: 40 percent / CH₂Cl₂

3.1: 95 percent / sodium hydride / dimethylformamide; various solvent(s) / 4 h / 20 °C

With dipyridinium dichromate; n-butyllithium; acetic anhydride; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo051012b