(E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

Base Information

Chemical Name:(E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester
CAS No.:161260-69-1
Molecular Formula:C₁₆H₁₈O₅
Molecular Weight:290.316
Hs Code.:

Synonyms:(E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

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Chemical Property of (E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

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Technology Process of (E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

There total 1 articles about (E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 153062-67-0
(3R)-3-(4,4-dimethyl-2-oxotetrahydrofuranyl) (E)-2-diazo-4-phenyl-3-butenoate

: (E)-(R)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

: 161260-69-1
(E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

Guidance literature:: With dirhodium tetraacetate; water; In diethyl ether; for 4h; Ambient temperature;
DOI:10.1021/jo961952j

Reference yield: 80.0%

: 161260-69-1
(E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

: (S)-2-Hydroxy-4-phenyl-butyric acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; Ambient temperature;
DOI:10.1021/jo961952j

Reference yield:

: 161260-69-1
(E)-(S)-2-Hydroxy-4-phenyl-but-3-enoic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester

: 115016-95-0,111611-91-7
(S)-2-hydroxy-4-phenylbutanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / H₂ / Pd-C / methanol / 3 h / Ambient temperature

2: LiOOH / tetrahydrofuran / 1 h / 0 °C

With lithium hydroperoxide; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jo961952j