(5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester

Base Information

• Chemical Name: (5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester
• CAS No.: 119506-57-9
• Molecular Formula: C₂₃H₁₇FN₄O₅
• Molecular Weight: 448.41

Synonyms:(5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester

Chemical Property of (5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester

There total 2 articles about (5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Nitrophenyl chloroformate (7693-46-1) + 3(S)-amino-1,3-dihydro-1-methyl-5-(2-fluorophenyl)-2H-1,4-benzodiazepin-2-one (209985-36-4) → (5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester (119506-57-9)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1021/jm00078a018

Reference yield:

→ (5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester (119506-57-9)

Guidance literature:

Reference yield:

(5-(2-Fluorophenyl)-2,3-dihydro-1-methyl-2-oxo-1H-1,4-benzodiazepin-3-yl)-carbamic acid-4-nitrophenyl ester (119506-57-9) → [5-(2-Fluoro-phenyl)-1-methyl-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl]-urea

Guidance literature:

With ammonia; triethylamine; In N,N-dimethyl-formamide; at 23 ℃; for 2h; Yield given;

DOI:10.1021/jm00078a018

upstream raw materials:

4-Nitrophenyl chloroformate

3(S)-amino-1,3-dihydro-1-methyl-5-(2-fluorophenyl)-2H-1,4-benzodiazepin-2-one

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