(E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

Base Information

Chemical Name:(E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate
CAS No.:1403783-37-8
Molecular Formula:C₃₄H₄₀O₃
Molecular Weight:496.69
Hs Code.:

Synonyms:(E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

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Chemical Property of (E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

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Technology Process of (E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

There total 4 articles about (E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-cyclohexyl-1-(4-ethylphenyl)-1-ethanone

: 114031-67-3
[4-(4-hydroxybenzoyl)phenyl]-2,2-dimethyl propanoate

: 1403783-37-8
(E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

: C₃₄H₄₀O₃

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; for 5h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.08.089

Reference yield:

: 4748-78-1
4-ethylbenzylaldehyde

: 1403783-37-8
(E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

: C₃₄H₄₀O₃

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 3 h / 0 °C

2: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1 h / 0 - 20 °C

3: titanium tetrachloride; zinc / tetrahydrofuran / 5 h / Inert atmosphere; Reflux

With sulfur trioxide pyridine complex; titanium tetrachloride; dimethyl sulfoxide; triethylamine; zinc; In tetrahydrofuran; dichloromethane; 3: |McMurry Reaction;
DOI:10.1016/j.tet.2012.08.089

Reference yield:

: 1284865-50-4
2-cyclohexyl-1-(4-ethylphenyl)ethanol

: 1403783-37-8
(E)-4-(3-cyclohexyl-2-(4-ethylphenyl)-1-(4-hydroxyphenyl)prop-1-enyl)phenyl-2,2-dimethylpropanoate

: C₃₄H₄₀O₃

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide; sulfur trioxide pyridine complex; triethylamine / dichloromethane / 1 h / 0 - 20 °C

2: titanium tetrachloride; zinc / tetrahydrofuran / 5 h / Inert atmosphere; Reflux

With sulfur trioxide pyridine complex; titanium tetrachloride; dimethyl sulfoxide; triethylamine; zinc; In tetrahydrofuran; dichloromethane; 2: |McMurry Reaction;
DOI:10.1016/j.tet.2012.08.089